Customization: | Available |
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CAS No.: | 93-98-1 |
Formula: | C13h11no |
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BENZANILIDE Chemical Properties |
Melting point | 161-163 °C(lit.) |
Boiling point | 117 °C10 mm Hg(lit.) |
density | 1,315 g/cm3 |
refractive index | 1.6050 (estimate) |
Fp | 117°C/10mm |
storage temp. | Store below +30°C. |
solubility | H2O: insoluble |
pka | 13.52±0.70(Predicted) |
form | Powder |
Colour Index | 42095 |
color | Grayish to yellow-green |
Water Solubility | Insoluble |
Merck | 14,1061 |
BRN | 1102980 |
CAS DataBase Reference | 93-98-1(CAS DataBase Reference) |
NIST Chemistry Reference | N-Phenylbenzoic acid amide(93-98-1) |
EPA Substance Registry System | Benzanilide (93-98-1) |
Safety Information |
Hazard Codes | Xn |
Risk Statements | 20/21/22-36/37/38 |
Safety Statements | 22-24/25-36-26 |
WGK Germany | 3 |
TSCA | Yes |
HS Code | 29242990 |
MSDS Information |
Provider | Language |
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SigmaAldrich | English |
ACROS | English |
ALFA | English |
BENZANILIDE Usage And Synthesis |
Chemical Properties | greyish to yellow-green powder |
Uses | manufacture of dyes and perfumes. |
Synthesis Reference(s) | Journal of Heterocyclic Chemistry, 24, p. 187, 1987 DOI: 10.1002/jhet.5570240135 The Journal of Organic Chemistry, 20, p. 1482, 1955 DOI: 10.1021/jo01128a004 Tetrahedron Letters, 31, p. 1063, 1990 DOI: 10.1016/S0040-4039(00)94431-9 |
Purification Methods | Crystallise benzanilide from pet ether (b 70-90o) using a Soxhlet extractor, and dry it overnight at 120o. Also crystallise it from EtOH. [Beilstein 12 IV 417.] |