Customization: | Available |
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Type: | Pharmaceutical Intermediates |
Appearance: | Crystal |
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Product Name: | 2,3,4,6-Tetra-O-acetyl-alpha-D-galactopyranosyl bromide |
Synonyms: | acetobromo-ó-d-galactose;alpha-d-galactopyranosylbromide,tetraacetate;2,3,4,6-Tetra-O-acetyl-a-D-galacopyranosyl bromide;BroMo 2,3,4,6-Tetra-O-acetyl-α-D-galactopyranoside (Stabilized with 2% (wt/wt) CaCO3);tetra-O-acetyl-alpha-D-galactopyranosyl bromide;2,3,4,6-Tetra-O-acetyl-alpha-D-galactopyranosyl bromide;Acetobromo-alpha-D-galactose;acetobromo-D-galactose;ACETOBROMO-A-D-GALACTOSE |
CAS: | 3068-32-4 |
MF: | C14H19BrO9 |
MW: | 411.2 |
EINECS: | 221-324-0 |
Product Categories: | Sugars, Carbohydrates & Glucosides;13C & 2H Sugars;Carbohydrates & Derivatives;substrate |
Mol File: | 3068-32-4.mol |
2,3,4,6-Tetra-O-acetyl-alpha-D-galactopyranosyl bromide Chemical Properties |
Melting point | 83-85 °C |
alpha | 210 º (c=3, CHCl3) |
Boiling point | 412.0±45.0 °C(Predicted) |
density | 1.7028 (rough estimate) |
refractive index | 1.4490 (estimate) |
storage temp. | Inert atmosphere,Store in freezer, under -20°C |
Water Solubility | Sparingly soluble |
BRN | 96671 |
Stability: | Temperature Sensitive; Store in freezer; Stabilized with 2% CaCO3 |
CAS DataBase Reference | 3068-32-4(CAS DataBase Reference) |
Safety Information |
Hazard Codes | Xi |
Risk Statements | 36/37/38 |
Safety Statements | 26-36-37/39 |
WGK Germany | 3 |
F | 8-10-21 |
HS Code | 29329990 |
MSDS Information |
2,3,4,6-Tetra-O-acetyl-alpha-D-galactopyranosyl bromide Usage And Synthesis |
Chemical Properties | White Crystalline Solid |
Uses | Temperature and moisture sensitive; Store in freezer; Stabilized with 2% CaCO3 |
Purification Methods | Purify acetobromo-D-galactose as for the glucose analogue (next entry). If the compound melts lower than 87o or is highly coloured, then dissolve it in CHCl3 (ca 3 volumes) and extract with H2O (2 volumes), 5% aqueous NaHCO3, and again with H2O and dry it over Na2SO4. Filter and evaporate it in a vacuum. The partially crystalline solid or syrup is dissolved in dry Et2O (must be very dry) and recrystallised by adding pet ether (b 40-60o) to give a white product. [McKellan & Horecker Biochemical Preparations 11 111 1960, Beilstein 17/6 V 369.] |
2,3,4,6-Tetra-O-acetyl-alpha-D-galactopyranosyl bromide Preparation Products And Raw materials |
Preparation Products | 3,4,6-Tri-O-acetyl-D-galactal-->D-Galactal |